Structural, Optical, and Magnetic Properties of Nickel Oxide Nanoparticles Through Precipitation Method
Keywords:
NiO NPS, precipitation method, XRD, VSM
Abstract
Nickel oxide nanoparticles (NiO NPS) have been prepared via chemical precipitation method. In this work, we are studying about the structural, morphological, and magnetic properties. The NiO NPS are characterized by different ways like XRD, SEM/EDX, FTIR, Antibacterial and VSM analysis. XRD indicates that the FCC structure of NiO NPS, with the crystallite size from 17.89 nm to 52.37 nm. The spherical shape was observed in SEM image. The basic composition of NiO NPS is determined by using the EDX. FTIR gives two wide peaks appeared at 421and 481 cm−1 due to Ni–O stretching vibration clearly indicates the formation of NiO at 600oC and 800oC. The VSM results demonstrate that the NiO NPS showing weak ferromagnetic behavior at 600 oC and 800 oC temperature.
References
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Karthik K, KalaiSelvan G, Kanagaraj M, Arumugam N S and Victor Jaya Particle size effect on the magnetic properties of NiO nanoparticles prepared by a precipitation method-. J. Alloys Compd. 509, 181–184 (2011)
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Al Boukhari J, Zeidan L, Khalaf A and Awad R Synthesis, Characterization, Optical and Magnetic Properties of Pure and Mn, Fe and Zn doped NiO Nanoparticles, Chemical Physics (2018), doi: https://doi.org/10.1016/j.chemphys.2018.07.046
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Hironari S, Nakano Y, Matsushita H, Onoe A, Kanai H and Yamashita Y Nanoparticle Ni and NiO: synthesis, characterization and magnetic properties.J.Mater. Synth. Process. 6, (1998). 415–420
Gates B C Supported metal clusters: synthesis, structure, catalysis.Chem. Rev.95, (1995).511-522
Lewis L N Chemical catalysis by colloids and clusters. Chem.Rev. 93, (1993) 2693–2730
Beecroft L L and Ober C K Nanocomposite materials for optical applications. Chem. Mater. 9, (1997) 1302–1317
Morup S in Studies of Superparamagnetism in Samples of Ultrafine Particles, Nanomagnetism, ed. by A. Hernando (KluwerAcademic Publishers, Boston, 1993), pp. 93– 99
Aharoni A in Introduction to the Theory of Ferromagnetism (Oxford University Press, New York, 1996), pp. 133–152
Nurul Nadia MohdZorkipli, Noor HaidaMohdKaus, and Ahmad AzminMohamad Synthesis of NiO Nanoparticles through Sol-gel Method Procedia Chemistry 19 ( 2016 ) 626 – 631
Shahverd A R, Nanomedicine: Nanotechnology, Biology and Medicine. 3(2007) 168- 171
Alagiri M, ponnusamy S, and Muthamizhchelvan C Journal of Master Electron (2012) 23,728-732.
SubhashThota and Jitendra Kumar, Journal of physics and chemistry of solids (2007) 68, 1951-1964.
AnandhaBabu G, Ravi G, Navaneethan, Arivanandhan M M, and Hayakawa Y, Journal of Mater sci: Master Electron (2014) 25, 5231-5240.
Mishra A K, Bandyopadhyay S and Das D Journal of Materials Research Bulletin (2012) 47, 2288-2293.
Miaomiao Liu, Jie Chang, Jing sun and LianGao Journal of ElecrochimicaActa (2013) 107, 9-15.
Mohammadijoo M, NaderiKhorshidi Z, Sadrnezhaad S K and Mazinani V Journal of Nanoscience and Nanotechnology (2014) 4(1), 6-9.
Kiani M A, AbbasniaTehrani M and Sayahi H Journal of AnalyticachimicaActa (2014) 839, 26-33.
Shaohui Liu, JianfengJia, Jiao Wang, Shijiang Liu, Xinchang Wang, Honghang Song, and Xing Hu Journal of Magnetism and Magnetic Materials (2012) 324, 2070-2074.
Sohaib Z Khan, Yudie Yuan, Amin Abdolvand, Marc schmidt, Philip Crouse, Lin Li, Zhu Liu, Martin Sharp and Watkins K G, Journal of Nanoparticle Research (2009) 11(14), 21-1427.
Manoharan C, Jothibas M, Johnson Jeyakumar S and Dhanapandian S Structural, optical and electrical properties of Zr-doped In2O3 thin films. Spectrochim. Acta Part A 145, 47–53 (2015)
Prince Richard J, KartharinalPunithavathy I, Johnson Jeyakumar S, Jothibas M and Praveen P Effect of morphology in the photocatalytic degradation of methyl violet dye using ZnOnanorods. J. Mater. Sci: Mater. Electron. 28(5), 4025–4034 (2017)
Zhiqiang Wei, HongxiaQiao, Hua Yang, cairong Zhang and Xiaoyan Yan Journal of Alloys and compounds (2009) 479, 855-858
Hassanpour M, Safardoust H and Ghanbari D J. Mater. Sci. Mater. Electron. 27, 2718–2727 (2016)
Mansournia M and Moradinia E J. Mater. Sci. Mater. Electron. 27, 82–89 (2016)
Ashok kumar M and Muthukumaran S Journal of Alloys and Compounds, (2014) 587,606-612
Wei Z, Qiao H, Yang H, Zhang C and Yan X Characterization of NiO nanoparticles by anodic arc plasma method. J Alloy Compd., 2009, 497, 855–858
Kavitha B, Nirmala M and Pavithra A Annealing effect on nickel oxide nanoparticles synthesized by sol-gel method. WSN 52 (2016) 118–129
Zook J M, Maccuspie R I, Locascio L E, Halter M D and Elliott J 2011 Stable nanoparticle aggregates/agglomerates of different sizes and the effect of their size on hemolytic cytotoxicity Nanotoxicology 5 517–30
Anandan K and Rajendran V Effects of Mn on the magnetic and optical properties and photocatalytic activities of NiO nanoparticles synthesized via the simple precipitation process. Mater. Sci. Eng. B 199, 48–56 (2015)
Karthik K, KalaiSelvan G, Kanagaraj M, Arumugam N S and Victor Jaya Particle size effect on the magnetic properties of NiO nanoparticles prepared by a precipitation method-. J. Alloys Compd. 509, 181–184 (2011)
Nandapure B I, Kondawar S B, Salunkhe M Y and Nandapure A I Magnetic and transport properties of conducting polyaniline/ nickel oxide nanocomposites. Adv. Mat. Lett. 4(2), 134–140(2013)
Balamurugan S, Linda Philip A J and Vidya R S A Versatile Combustion Synthesis and Properties of Nickel Oxide (NiO) Nanoparticles, J Supercond Nov Magn 2017
Al Boukhari J, Zeidan L, Khalaf A and Awad R Synthesis, Characterization, Optical and Magnetic Properties of Pure and Mn, Fe and Zn doped NiO Nanoparticles, Chemical Physics (2018), doi: https://doi.org/10.1016/j.chemphys.2018.07.046
Ezhilarasi A A, Vijaya J J, Kaviyarasu K, Kennedy L J, Ramalingam R J, Al- Lohedan H A, J. Photochem. Photobiol. B. Biol. 180 (2018)39-50
Published
2021-04-23
How to Cite
S.Sivakumar, & Nazir Ahmad Mala. (2021). Structural, Optical, and Magnetic Properties of Nickel Oxide Nanoparticles Through Precipitation Method. Central Asian Journal of Medical and Natural Science, 2(2), 240-249. https://doi.org/10.17605/cajmns.v2i2.159
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